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Fundamentals of Analytical Chemistry

Code: 40343
ECTS: 5.0
Lecturers in charge: doc. dr. sc. Ivan Nemet
Lecturers: doc. dr. sc. Ivan Nemet - Seminar

Nikolina Beljan , mag. chem. - Practicum
doc. dr. sc. Ivan Nemet - Practicum
Take exam: Studomat
English level:

0,0,0

The lecturer is not able to offer courses in English at this time.
Load:

1. komponenta

Lecture typeTotal
Lectures 30
Practicum 45
Seminar 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
LEARNING OUTCOMES:
1. To describe basic classification of analytical chemistry methods
2. To apply qulitative analytical techniques in model sample analysis
3. To explain principal characteristics of titrimetric methods
4. To apply titrimetric techniques in quantitative determination of selected analytes
5. To classify instrumental methods according to interaction of radiation and matter
6. To describe analytical characteristics of selected atomic spectrometry methods
7. To describe analytical characteristics of selected molecular spectroscopy methods
8. To apply instrumental analytical techniques in real sample analysis
COURSE CONTENT:
LECTURES
1. Analitics: sample, analyte, sampling, solution preparation
2. Gravimetry: basic concept, quantitative applications
3. Titrimetry: primary and secondary standards, final point determination
4. Acid-base titrations
5. Complexometry
6. Precipitation titrations
7. Redox titrations
8. Introduction in instrumental analysis
9. Atomic absorption spectrometry
10. Atomic emission spectrometry
11. UV/VIS spectrophotometry
12. Vibrational methods (IR and Raman spectroscopy)
13. Nuclear magnetic resonance
SEMINARS: problem solving following the lecture unit
LABORATORY EXERCISES:
1. Qualitative analysis of biological important analytes (Cu, Fe, Na, K, NO3 -, NO2-, organic amines, urea)
2. Chemical analysis of soil ( gravimetry of groups)
3. Kjeldahl analysis of nitrogen ( acid-base titrations)
4. Determination of organic constituents in water (redox titrations)
5. Determination of phosphates by UV/VIS spectrophotometry
6. Analysis of kidney stones (vibrational spectroscopy)
7. Flame photometric determination of sodium (atomic spectrometry)
Literature:
  1. 1) D. A. Skoog, D. M. West i F. J. Holler, Osnove analitičke kemije, Školska knjiga, Zagreb, 1998.
  2. 1) F. J. Holler, D. A. Skoog, and S.R. Crouch, Principles of Instrumental Analysis, 6th Ed., Thomson, Belmont, 2007.
    2) M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga-Zagreb, 2003.
3. semester
Izborni predmeti - Regular study - Biology
Consultations schedule: